HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 10141432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Trifluoromethanesulfonyl chloride | HCID 79000 | — |
| Reactant | HCID 22388582 | HCID 22388582 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10141432 | HCID 10141432 | 11% |
Reaction Steps
The final title compound (23 mg, 11%) was prepared from (2-{4-[4-(aminomethyl)phenyl]phenoxy}propyl)[(methylethyl)sulfonyl]amine hydrochloride (150 mg, 0.430 mmol, prepared in example 32) methylene chloride 2.5 mL, anhydrous) triethylamine (0.07 mL, 0.471 mmol) and trifluoromethylsulfonyl chloride (9.06 mL, 0.565 mmol), in a manner analogous to Example 29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06911476B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-3a464d6e860b4802a61377ead5bc6bc3 |
| Source note | uspto-grants-2005_06 |