Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1072676Generated: November 1, 2026

Triethylamine → HCID 10141432, compound

https://huagongshe.com/reaction/1072676

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantTrifluoromethanesulfonyl chlorideHCID 79000—
ReactantHCID 22388582HCID 22388582—
SolventDichloromethaneHCID 6344—
ProductHCID 10141432HCID 1014143211%

Reaction Steps

The final title compound (23 mg, 11%) was prepared from (2-{4-[4-(aminomethyl)phenyl]phenoxy}propyl)[(methylethyl)sulfonyl]amine hydrochloride (150 mg, 0.430 mmol, prepared in example 32) methylene chloride 2.5 mL, anhydrous) triethylamine (0.07 mL, 0.471 mmol) and trifluoromethylsulfonyl chloride (9.06 mL, 0.565 mmol), in a manner analogous to Example 29.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06911476B2
Source datasetuspto-grants-2005_06
ORD IDord-3a464d6e860b4802a61377ead5bc6bc3
Source noteuspto-grants-2005_06