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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1072677Generated: November 2, 2026

Triethylamine → HCID 10224776, compound

https://huagongshe.com/reaction/1072677

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantIsobutyryl chlorideHCID 62325—
ReactantHCID 22388582HCID 22388582—
SolventDichloromethaneHCID 6344—
ProductHCID 10224776HCID 1022477619%

Reaction Steps

The final title compound (59 mg, 19%) was prepared from (2-{4-[4-(aminomethyl)phenyl]phenoxy}propyl)[(methylethyl)sulfonyl]amine hydrochloride (250 mg, 0.717 mmol, prepared in example 32) methylene chloride (4.6 mL, absolute) triethylamine (0.07 mL, 0.8621 mmol), aind isobutyryl chloride (0.06 mL, 1.0345 mmol), in a manner analogous to Example 29.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06911476B2
Source datasetuspto-grants-2005_06
ORD IDord-9188f855073346b3a30dce517662cd3f
Source noteuspto-grants-2005_06