HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 10224776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Isobutyryl chloride | HCID 62325 | — |
| Reactant | HCID 22388582 | HCID 22388582 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10224776 | HCID 10224776 | 19% |
Reaction Steps
The final title compound (59 mg, 19%) was prepared from (2-{4-[4-(aminomethyl)phenyl]phenoxy}propyl)[(methylethyl)sulfonyl]amine hydrochloride (250 mg, 0.717 mmol, prepared in example 32) methylene chloride (4.6 mL, absolute) triethylamine (0.07 mL, 0.8621 mmol), aind isobutyryl chloride (0.06 mL, 1.0345 mmol), in a manner analogous to Example 29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06911476B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-9188f855073346b3a30dce517662cd3f |
| Source note | uspto-grants-2005_06 |