Triethylamine → HCID 22387601, compound

Participants

Reaction Steps

To a solution of 3-(4-butylphenyl)propanol (2.86 g, 14.9 mmol) and triethylamine (1.51 g, 14.9 mmol) in ethyl acetate (30 ml) was added methanesulfonyl chloride (1.70 g, 14.9 mmol) and the mixture was stirred at room temperature for 2 hours. The reaction solution was washed with water and saturated brine, dried over magnesium sulfate anhydride and concentrated under reduced pressure to give the object compound as an oily substance. 4.02 g (yield: 100%)

Provenance & Evidence