HRID1072724

反应详情

EQUATION

反应方程式

HRID 1072724 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of (2R)-2-([4-[1-(4-pentylphenylethyl)-5-methyl-1H-pyrrol-2-yl]phenyl]oxy)-3-phenylpropanoic acid (615 mg, 1.24 mmol) in ethanol (10 ml) was added 1N sodium hydroxide-ethanol (1.21 ml, 1.21 mmol) and the mixture was concentrated. To the residue was added hexane to give the object compound as a solid. 500 mg, (yield 62%)

WORKUP

后处理

  1. concentrationthe mixture was concentrated
  2. additionTo the residue was added hexane