HRID1072731
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of ethyl (2E)-3-(1-naphthyl)propenoate (37.6 g, 166 mmol) in ethanol (500 ml) was added 10% palladium carbon (4 g) and the mixture was stirred under hydrogen atmosphere for 5 hours. The insoluble matter was filtered out and the filtrate was concentrated to give the object compound as an oily substance. 37.7 g (yield: 99.7%)
WORKUP
后处理
- filtrationThe insoluble matter was filtered out
- concentrationthe filtrate was concentrated
- customto give the object compound as an oily substance