HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl (2E)-3-(1-naphthyl)propenoate → Ethyl 3-(1-naphthyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl (2E)-3-(1-naphthyl)propenoate | HCID 11218397 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(1-naphthyl)propanoate | HCID 10966256 | 99.7% |
Reaction Steps
To a solution of ethyl (2E)-3-(1-naphthyl)propenoate (37.6 g, 166 mmol) in ethanol (500 ml) was added 10% palladium carbon (4 g) and the mixture was stirred under hydrogen atmosphere for 5 hours. The insoluble matter was filtered out and the filtrate was concentrated to give the object compound as an oily substance. 37.7 g (yield: 99.7%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06911468B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-baa84f75ecec4bf19d7a1fdb5b57d4b2 |
| Source note | uspto-grants-2005_06 |