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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1072738Generated: November 3, 2026

Ethanol → HCID 22387303, compound

https://huagongshe.com/reaction/1072738

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantHCID 22387316HCID 22387316—
CatalystHCID 178418390HCID 178418390—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22387303HCID 2238730393.5%

Reaction Steps

To a solution of 2-(4-benzyloxyphenyl)-1-(4-decyloxyphenyl)-5-methyl-1H-pyrrole (1.70 g, 3.43 mmol) in ethanol (60 ml) and tetrahydrofuran (30 ml) was added 10% palladium carbon (200 mg) and the mixture was stirred for 4 hours under hydrogen atmosphere. The insoluble matter was filtered out and the filtrate was concentrated to give the object compound as an oily substance. 1.30 g (yield: 93.5%)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06911468B2
Source datasetuspto-grants-2005_06
ORD IDord-3520b9ffeb1344818a66f30bc9efee13
Source noteuspto-grants-2005_06