HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 86759780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69731997 | HCID 69731997 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86759780 | HCID 86759780 | 82.9% |
Reaction Steps
Ethanol (6 ml) and a solution of 1N sodium hydroxide in ethanol (1.10 ml) were added to (2R)-2-(4-{5-methyl-1-[3-(4-pentylphenoxy)propyl]-1H-pyrrol-2-yl}phenoxy)-3-phenylpropanoic acid (640 mg, 1.22 mmol) and the mixture was concentrated. To the residue was added diisopropylether to give the object compound as a solid. 499 mg (yield: 82.9%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06911468B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-e0c970753b0342fc9ac70712123b6327 |
| Source note | uspto-grants-2005_06 |