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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1072759Generated: November 3, 2026

HCID 22387492, compound → HCID 22387306, compound

https://huagongshe.com/reaction/1072759

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22387492HCID 22387492—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22387306HCID 2238730693.3%

Reaction Steps

To a solution of 2-(4-benzyloxyphenyl)-1-(4-decylphenyl)-5-methyl-1H-pyrrole (2.77 g, 5.77 mmol) in methanol (40 ml) and tetrahydrofuran (40 ml) was added 10% palladium carbon (200 mg) and the mixture was stirred for 4 hours under hydrogen atmosphere. The insoluble matter was filtered out and the filtrate was concentrated to give the object compound as an oily substance. 2.10 g (yield: 93.3%)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06911468B2
Source datasetuspto-grants-2005_06
ORD IDord-fa9d888ed9a741bc86271cd21b680b03
Source noteuspto-grants-2005_06