HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22387492, compound → HCID 22387306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22387492 | HCID 22387492 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22387306 | HCID 22387306 | 93.3% |
Reaction Steps
To a solution of 2-(4-benzyloxyphenyl)-1-(4-decylphenyl)-5-methyl-1H-pyrrole (2.77 g, 5.77 mmol) in methanol (40 ml) and tetrahydrofuran (40 ml) was added 10% palladium carbon (200 mg) and the mixture was stirred for 4 hours under hydrogen atmosphere. The insoluble matter was filtered out and the filtrate was concentrated to give the object compound as an oily substance. 2.10 g (yield: 93.3%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06911468B2 |
| Source dataset | uspto-grants-2005_06 |
| ORD ID | ord-fa9d888ed9a741bc86271cd21b680b03 |
| Source note | uspto-grants-2005_06 |