Glyoxal → HCID 15099950, compound

HRID 1073038Notes

Reaction equation

HRID 1073038 reaction equation
[CH2:1]([PH2:4])[CH2:2][CH3:3].[CH:5]([CH:7]=[O:8])=[O:6]>O1CCCC1>[CH2:1]([P:4]1[CH:5]([OH:6])[CH:7]([OH:8])[P:4]([CH2:1][CH2:2][CH3:3])[CH:5]([OH:6])[CH:7]1[OH:8])[CH2:2][CH3:3]

Participants

4

Reactant 2

HCID 7860GlyoxalHCID 14647240Propylphosphane

Product 1

HCID 15099950HCID 15099950, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Following the procedure of Example 1, mono-n-propylphosphine, in tetrahydrofuran, as solvent, is reacted with a 40% aqueous glyoxal solution, to give 1,4-di-n-propyl-2,3,5,6-tetrahydroxy-1,4-diphosphorinane, a solid melting at 131°-133° C.

Sources & evidence

ORD record
ord-f4bd52364dba460db12d0ce28ebd9c72
Source dataset
uspto-grants-1990_11
Patent number
US04968416

Reaction notes

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