Silver Nitrate → N-vinyl-2-pyrrolidone

HRID 1073045Notes

Reaction equation

HRID 1073045 reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]2[NH:6][N:7]=[N:8][C:4]=2[CH:3]=1.[N+]([O-])([O-])=[O:12].[Ag+:15].[Na].S(C1[C:29]2[N:28]=NN[C:25]=2[CH:24]=[CH:23]C=1)(O)(=O)=O>>[Ag:15].[CH3:1][C:2]1[CH:10]=[CH:9][C:5]2[NH:6][N:7]=[N:8][C:4]=2[CH:3]=1.[CH2:10]=[CH:2][N:28]1[C:29](=[O:12])[CH2:25][CH2:24][CH2:23]1

Participants

5

Reactant 3

HCID 24470Silver NitrateHCID 178423511HCID 178423511, compoundHCID 178527607HCID 178527607, compound

Product 2

HCID 6917N-vinyl-2-pyrrolidoneHCID 178423512HCID 178423512, compound

Procedure

28.8 g of 5-methylbenzotriazole silver salt obtained by reaction of 5-methylbenzotriazole and silver nitrate in water-alcohol mixed solvent, 16.0 g of poly (N-vinyl pyrrolidone) and 1.33 g or 4-sulfobenzotriazole sodium salt were dispersed with alumina ball mill. This solution was arranged to have pH of 5.5 and quantity of 200 ml.

Sources & evidence

ORD record
ord-c9e519a474374f3eb9347a940a79b9d4
Source dataset
uspto-grants-1990_11
Patent number
US04968597

Reaction notes

Loading…