Hydrochloric Acid → HCID 14181207, compound

HRID 1073118Notes

Reaction equation

HRID 1073118 reaction equation
[CH2:1]([N:4]([CH2:17][CH2:18][CH3:19])[CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([CH2:15][NH2:16])[CH:9]=[CH:10][CH:11]=2)[CH2:6]1)[CH2:2][CH3:3].[ClH:20]>CCOCC>[ClH:20].[CH2:17]([N:4]([CH2:1][CH2:2][CH3:3])[CH:5]1[CH2:14][CH2:13][C:12]2[C:7](=[C:8]([CH2:15][NH2:16])[CH:9]=[CH:10][CH:11]=2)[CH2:6]1)[CH2:18][CH3:19]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 14181206HCID 14181206, compound

Product 1

HCID 14181207HCID 14181207, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The compound of Example 12 was dissolved in ether. By dropwise addition of ethereal hydrogen chloride solution, the hydrochloride was precipitated and was then filtered off under suction and dried in vacuo at room temperature.

Workup

  1. customthe hydrochloride was precipitated
  2. filtrationwas then filtered off under suction
  3. customdried in vacuo at room temperature

Sources & evidence

ORD record
ord-8db367c36fa74148b5f4696d5c67a3db
Source dataset
uspto-grants-1990_11
Patent number
US04968679

Reaction notes

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