Water → HCID 54526511, compound

HRID 1073134Notes

Reaction equation

HRID 1073134 reaction equation
C([NH:9][C:10]([N:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:23]=[CH:22][C:21]([C:24]3[CH:25]([CH3:31])[CH2:26][C:27](=[O:30])[NH:28][N:29]=3)=[CH:20][C:19]=2[N+:32]([O-:34])=[O:33])[CH2:14][CH2:13]1)=[S:11])(=O)C1C=CC=CC=1.O.C(=O)([O-])[O-].[K+].[K+]>CO>[NH2:9][C:10]([N:12]1[CH2:17][CH2:16][N:15]([C:18]2[CH:23]=[CH:22][C:21]([C:24]3[CH:25]([CH3:31])[CH2:26][C:27](=[O:30])[NH:28][N:29]=3)=[CH:20][C:19]=2[N+:32]([O-:34])=[O:33])[CH2:14][CH2:13]1)=[S:11]

Participants

5

Reactant 3

HCID 962WaterHCID 11430Potassium CarbonateHCID 53784822HCID 53784822, compound

Product 1

HCID 54526511HCID 54526511, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

66.6 g (0.139 mol) of the compound synthesized as described under (a) are boiled under reflux in 1200 ml of methanol and 150 ml of water in the presence of 21.6 g (0.156 mol) of potassium carbonate.

Sources & evidence

ORD record
ord-4c69faf05f4d4b2da6f25e0c25291e87
Source dataset
uspto-grants-1990_11
Patent number
US04968683

Reaction notes

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