HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22158384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 3-Formyl-2-ethylimidazo[2,1-b]benzothiazole | HCID 22158396 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22158384 | HCID 22158384 | 63.4% |
Reaction Steps
Furthermore, 3.88 g of 3-formyl-2-ethylimidazo[2,1-b]benzothiazole was suspended in 30 ml of methanol and 1.0 g of sodium borohydride was added to the suspension followed by refluxing for one hour. After completion of the reaction, the reaction solution was evaporated to dryness and the residue was washed with water. The crystals obtained were recrystallized from ethanol to give 2.48 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04968708 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-96418546548d42a68d0f07f4f2f8d39d |
| Source note | uspto-grants-1990_11 |