Dimethylformamide → HCID 22158380, compound

Participants

Reaction Steps

In 50 ml of dry dimethylformamide was suspended 3.00 g of 2-methylimidazo[2,1-b]benzothiazole-3-methanol. Then, 1.12 g of 60% sodium hydride was added to the suspension. After stirring for 30 minutes, 3.00 g of o-methoxybenzoyl chloride was added to the mixture followed by stirring at room temperature for 3 hours. Ice water was added to the reaction solution and the system extracted with chloroform. After the chloroform was removed, 2.60 g of the title compound was obtained.

Provenance & Evidence