Bromide ion → HCID 131716686, compound

Participants

Reaction Steps

To a suspension of 3.53 g of 1-[2-oxo-2-[4(phenylthio)phenyl]ethyl]-3,5,7-triaza-1-azoniatricyclo[3.3.1.13,7 ]decane, bromide in 35 ml of ethanol was added 6 ml of concentrated hydrochloric acid. This mixture was stirred for 17 hours, then the solid was collected and washed with ethanol and ether. This solid was stirred with 15 ml of water at 0° C. for 50 minutes, then the solid was collected, washed with 20 ml of ice cold water and dried, giving 1.38 g of the desired compound as a white solid, mp 222°-224° C. (dec.).

Provenance & Evidence