HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 15085981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 5-chloro-1H-indole-2,3-dione | HCID 87203 | — |
| Reactant | HCID 22158358 | HCID 22158358 | — |
| Product | HCID 15085981 | HCID 15085981 | — |
Reaction Steps
A basic aqueous solution of 4.54 g of 5-chloroisatin in water was reacted with 9.0 g of 2-amino-1-(4'-fluoro-[1,1'-biphenyl]-4-yl)ethanone hydrochloride by the procedure described in example 20, giving 6.2 g of the desired compound as a yellow solid, mp 255°-257° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04968702 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-813b3791bfc04b4cbce32dd63e126e42 |
| Source note | uspto-grants-1990_11 |