Hydrogen Peroxide → HCID 54043075, compound

HRID 1073347Notes

Reaction equation

HRID 1073347 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][N:10]=2)[CH:6]=[CH:7][CH:8]=1)#[N:2].[OH:15]O>C(O)(=O)C>[C:1]([C:3]1[CH:4]=[C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][N+:10]=2[O-:15])[CH:6]=[CH:7][CH:8]=1)#[N:2]

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 4674258HCID 4674258, compound

Product 1

HCID 54043075HCID 54043075, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Starting from 2-(3-cyanophenyl)-pyridine, the title compound is prepared by oxidation with H2O2 in glacial acetic acid [J. Heterocycl. Chem. 11. 299 (974)].

Sources & evidence

ORD record
ord-a3518ac794314ea9b595463bd1177197
Source dataset
uspto-grants-1990_11
Patent number
US04968804

Reaction notes

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