HRID1073348

反应详情

EQUATION

反应方程式

HRID 1073348 的结构方程式

PROCEDURE

实验过程

Starting from 3-bromophenyllithium, 4-chloropyridine and chloroformic acid phenyl ester (for the acylation of the pyridine nitrogen), the title compound is prepared analogously to J. Org. Chem. 50, 4410 (1985). A corresponding 1-acyl-1,2-dihydropyridine is formed as intermediate and is aromatised by reaction with o-chloroanil ##STR23## to form the title compound. (b) 4-cyano-2-(3-cyanophenyl)-pyridine