HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibutylstannane → Bis[2-(2-ethylhexanoyloxy)ethyl]dibutyltin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibutylstannane | HCID 6513 | — |
| Reactant | Vinyl 2-ethylhexanoate | HCID 62343 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | Bis[2-(2-ethylhexanoyloxy)ethyl]dibutyltin | HCID 14512235 | — |
Reaction Steps
2.349 g (0.01 mol) of dibutyltin dihydride, 3.405 g (0.02 mol) of distilled vinyl 2-ethylhexanoate and 2.5 g of anhydrous cyclohexane were introduced into a Pyrex® tube. The exposure to ultraviolet rays was for 8 hours 30 min at 30°-35° C. The solvent was removed under vacuum at ambient temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04970115 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-afdeea21f83649c98c3d79d9bf899067 |
| Source note | uspto-grants-1990_11 |