Dimethylcarbamoyl Chloride → HCID 19893972, compound
Reaction equation
[C:1]([C:5]1[N:9]=[C:8]([S:10][CH2:11][C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)[NH:7][N:6]=1)([CH3:4])([CH3:3])[CH3:2].[CH3:17][N:18]([CH3:22])[C:19](Cl)=[O:20]>>[CH3:17][N:18]([CH3:22])[C:19]([N:7]1[C:8]([S:10][CH2:11][C:12]2[O:13][CH:14]=[CH:15][CH:16]=2)=[N:9][C:5]([C:1]([CH3:4])([CH3:2])[CH3:3])=[N:6]1)=[O:20]Participants
3
Procedure
3-t-Butyl-5-(fur-2-yl-methylthio)-1H-1,2,4triazole was reacted with dimethylcarbamoyl chloride by substantially the same procedure as described in Example 1 to yield 1-dimethylcarbamoyl-3-t-butyl-5-(fur-2-yl-methylthio)-1H-1,2,4-triazole, an oil.
Sources & evidence
- ORD record
- ord-52c947f785ac40eba8166dce6d560123
- Source dataset
- uspto-grants-1990_11
- Patent number
- US04970224
Reaction notes
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