HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 10094518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | N,N-Diethyl-2-piperidinemethanamine | HCID 254287 | — |
| Reactant | HCID 14075459 | HCID 14075459 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 10094518 | HCID 10094518 | 54% |
Reaction Steps
Prepared in analogy to Example 2 from 11-(chloroacetyl)-5,11-dihydro-8-methyl-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 2-[(diethylamino)methyl]piperidine, but using acetonitrile as solvent, in a yield of 54% of theory. M.p. 173-174° C. (diisopropylether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04971966 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-432754fce64e433a96372f2c16b39923 |
| Source note | uspto-grants-1990_11 |