Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 178507684 | HCID 178507684 | — |
| Product | HCID 178466987 | HCID 178466987 | — |
Reaction Steps
1.8 g of sodium are dissolved in 100 ml of ethanol. 10 g of 2,4-diamino-6-chloropyrimidine 3-oxide are added. The reaction mixture is refluxed until the starting material has disappeared and is heated to 120° C. in an autoclave for 7 hours. It is returned to ambient temperature and the insoluble material is filtered off and washed with ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04973474 |
|---|
| Source dataset | uspto-grants-1990_11 |
|---|
| ORD ID | ord-57b93f5ca486432fb7248bec06435744 |
|---|
| Source note | uspto-grants-1990_11 |
|---|
