Sodium → HCID 178493290, compound

HRID 1074126Notes

Reaction equation

HRID 1074126 reaction equation
[Na].[NH2:2][C:3]1[N+:8]([O-:9])=[C:7]([NH2:10])[CH:6]=[C:5]([O:11][C:12]2C=CC(Cl)=CC=2Cl)[N:4]=1>CO>[NH2:2][C:3]1[N+:8]([O-:9])=[C:7]([NH2:10])[CH:6]=[C:5]([O:11][CH3:12])[N:4]=1

Participants

4

Reactant 2

HCID 5360545SodiumHCID 178507931HCID 178507931, compound

Product 1

HCID 178493290HCID 178493290, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.8 g of sodium are dissolved in 150 ml of methanol. 15 of 2,4-diamino-6-(2,4-dichlorophenoxy)pyrimidine 3-oxide are added and the reaction mixture is refluxed for 15 days.

Workup

  1. temperaturethe reaction mixture is refluxed for 15 days

Sources & evidence

ORD record
ord-5478994d0ab047c3816fada093d2600e
Source dataset
uspto-grants-1990_11
Patent number
US04973474

Reaction notes

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