Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 14459254 | HCID 14459254 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14459255 | HCID 14459255 | — |
Reaction Steps
1.26 g (12.5 mmol) of phenyl isocyanate are used to a suspension of 3 g (12.5 mmol) of the compound from Example 2 in 30 ml of toluene and 1.5 g (12.5 mmol) of triethylamine are slowly added dropwise at 0° C. The mixture is stirred overnight at 25° C. The toluene phase is washed with water, the product precipitating out. After drying 3.54 g are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04973598 |
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| Source dataset | uspto-grants-1990_11 |
|---|
| ORD ID | ord-518b170b29c14136ae47260d50c32943 |
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| Source note | uspto-grants-1990_11 |
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