Hydrochloric Acid → HCID 22155982, compound

HRID 1074193Notes

Reaction equation

HRID 1074193 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[S:9][C:10]1[N:11]([CH3:15])[CH:12]=[CH:13][N:14]=1.Cl>CCOCC.ClCCl>[ClH:1].[Cl:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[C:3]=1[S:9][C:10]1[N:11]([CH3:15])[CH:12]=[CH:13][N:14]=1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 15077493HCID 15077493, compound

Product 1

HCID 22155982HCID 22155982, compoundYield 77%

Reagents, catalysts & solvents 2

HCID 3283Diethyl EtherSolventHCID 6344DichloromethaneSolvent

Procedure

The product from Example 17 was treated with hydrogen chloride in ether and dichloromethane to give a 77% yield of the product as colorless prisms, mp 211°-222° C.

Sources & evidence

ORD record
ord-160cb0e4c13e45549d1d034958c57e00
Source dataset
uspto-grants-1990_11
Patent number
US04973599

Reaction notes

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