Hydrochloric Acid → HCID 22155956, compound

HRID 1074195Notes

Reaction equation

HRID 1074195 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[N:10]([CH3:14])[CH:11]=[CH:12][N:13]=2)=[C:4]([N+:15]([O-:17])=[O:16])[CH:3]=1.Cl>ClCCl.CCOCC>[ClH:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[N:10]([CH3:14])[CH:11]=[CH:12][N:13]=2)=[C:4]([N+:15]([O-:17])=[O:16])[CH:3]=1

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 15077494HCID 15077494, compound

Product 1

HCID 22155956HCID 22155956, compound

Reagents, catalysts & solvents 2

HCID 3283Diethyl EtherSolventHCID 6344DichloromethaneSolvent

Procedure

The product from Example 19 was treated with hydrogen chloride in dichloromethane and ether to give the product as yellow prisms mp 155°-160° C.

Sources & evidence

ORD record
ord-2f200fbf9ca442f48ee8412b072d1953
Source dataset
uspto-grants-1990_11
Patent number
US04973599

Reaction notes

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