HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22155954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-[(4-Nitrophenyl)thio]-1H-imidazole | HCID 15077498 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22155954 | HCID 22155954 | — |
Reaction Steps
The product from Example 26 was dissolved in methanol and treated with an excess of hydrogen chloride in ethyl alcohol. The mixture was concentrated and the residue triturated with ether and filtered. The solid was recrystallized from methanol to give the product as colorless prisms, mp 235°-240° C. (sealed tube).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04973599 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-02409625d3164c6985dedd1c1d7c52dc |
| Source note | uspto-grants-1990_11 |