Hydrochloric Acid → HCID 22155954, compound

HRID 1074199Notes

Reaction equation

HRID 1074199 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][C:11]2[NH:12][CH:13]=[CH:14][N:15]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[ClH:16]>CO.C(O)C>[ClH:16].[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][C:11]2[NH:15][CH:14]=[CH:13][N:12]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 150774982-[(4-Nitrophenyl)thio]-1H-imidazole

Product 1

HCID 22155954HCID 22155954, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 887MethanolSolvent

Procedure

The product from Example 26 was dissolved in methanol and treated with an excess of hydrogen chloride in ethyl alcohol. The mixture was concentrated and the residue triturated with ether and filtered. The solid was recrystallized from methanol to give the product as colorless prisms, mp 235°-240° C. (sealed tube).

Workup

  1. concentrationThe mixture was concentrated
  2. customthe residue triturated with ether
  3. filtrationfiltered
  4. customThe solid was recrystallized from methanol
  5. customto give

Sources & evidence

ORD record
ord-02409625d3164c6985dedd1c1d7c52dc
Source dataset
uspto-grants-1990_11
Patent number
US04973599

Reaction notes

Loading…