HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22155962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-[(2-Chlorophenyl)thio]-1H-imidazole | HCID 15077500 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22155962 | HCID 22155962 | — |
Reaction Steps
A solution of the product from Example 33 in methanol was treated with an excess of hydrogen chloride in ethyl alcohol. The mixture was concentrated in vacuo and the residue triturated with ether and filtered. The solid was recrystallized from methanol/ether to give the product as colorless prisms, mp 189°-192° C. (sealed tube).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04973599 |
| Source dataset | uspto-grants-1990_11 |
| ORD ID | ord-d49466c87cf54f1ca4d630fe8988a6b2 |
| Source note | uspto-grants-1990_11 |