Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Mesityl oxide | HCID 8858 | — |
| Reactant | 4-Hydroxytamoxifen | HCID 449459 | — |
| Product | HCID 131716720 | HCID 131716720 | — |
Reaction Steps
0.1 mol of the 4-hydroxytamoxifen complexes from Examples (1c2) and 2 are introduced into 400 ml of mesityl oxide at 60° C. When the substance has dissolved, the solution is cooled to 15° C. and the precipitate obtained is suction filtered and washed with 75 ml of methyl tert.-butyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04973755 |
|---|
| Source dataset | uspto-grants-1990_11 |
|---|
| ORD ID | ord-e1cd44ffe13e4808b9031a637015b75a |
|---|
| Source note | uspto-grants-1990_11 |
|---|
