HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Dibromooct-1-yne → HCID 53878301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Dibromooct-1-yne | HCID 12831190 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53878301 | HCID 53878301 | — |
Reaction Steps
On the other hand, 1,8-dibromo-1-octyne and a copper halide as the catalyst are dissolved in tetrahydrofuran in a reaction vessel to form a reaction mixture, into which the above prepared Grignard reagent in tetrahydrofuran is added dropwise to effect the reaction between the reactants followed by hydrolysis and distillation to give 1-bromohexadeca-11-en-7-yne. The reaction is expressed by the following reaction equation:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04391984 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-d6e76ae3c9aa4b879d64848b41ad20b4 |
| Source note | uspto-grants-1983_07 |