Methylamine → HCID 20496074, compound
Reaction equation
[N+:1]([CH2:4][CH:5]([CH3:9])[CH:6](C)O)([O-:3])=[O:2].[CH3:10][NH2:11]>>[CH3:10][NH:11][CH2:6][CH:5]([CH2:4][N+:1]([O-:3])=[O:2])[CH3:9]Participants
3
Procedure
2-Nitromethylmethylpropanol is reacted with methylamine to form N-methyl-2-nitromethylpropylamine which is hydrogenated to the diamine. The latter is then reacted with acetic acid to form 1,2,4,4-tetramethyl-2-imidazoline. It is tested as a polyurethane foam catalyst by the method of Example 1 and is found to be effective.
Sources & evidence
- ORD record
- ord-5bf0d9670cbf4d83b6cb4bcd5620aa8d
- Source dataset
- uspto-grants-1983_07
- Patent number
- US04393149
Reaction notes
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