HCID 20496156, compound → HCID 20496154, compound

Participants

Reaction Steps

A mixture of N-methyl-3-nitro-4-trifluoromethylbenzenamine (20 g., 0.09 mole) and absolute alcohol (200 ml.) was reduced with 5% palladium on carbon 50% wet. The material absorbed 24 lbs. of hydrogen (100% theory) in 1 hr. The catalyst was removed by filtration and the filtrate stripped in vacuo. The dark oil crystallized to give 17 g. (99%). The material used as an intermediate in Part C.

Provenance & Evidence