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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1074597Generated: October 31, 2026

Dimethylformamide dimethyl acetal → HCID 54468687, compound

https://huagongshe.com/reaction/1074597

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamide dimethyl acetalHCID 78373—
ReactantN-(2-chlorophenyl)-2-cyanoacetamideHCID 693035—
ProductHCID 54468687HCID 54468687—

Reaction Steps

As for Example 1, 2'-chloro-2-cyanoacetanilide, white crystalline product, m.p. 122.5°-123° C. (prepared as described in U.S. Pat. No. 3,116,312), is heated with N,N-dimethylformamide dimethylacetal to give 2'-chloro-2-cyano-3-dimethylaminoacrylanilide as colorless prisms, m.p. 104°-105° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04393217
Source datasetuspto-grants-1983_07
ORD IDord-0e889a84c7b841bf9ba7a4acf16e03fa
Source noteuspto-grants-1983_07