HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 54542368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | N-(2-chloro-4-fluorophenyl)-2-cyanoacetamide | HCID 3644962 | — |
| Product | HCID 54542368 | HCID 54542368 | — |
Reaction Steps
As for Example 1, 2'-chloro-2-cyano-4'-fluoroacetanilide as colorless needles, m.p. 138°-139° C. (prepared by the procedure described in U.S. Pat. No. 3,116,312), is heated with N,N-dimethylformamide dimethylacetal to give 2'-chloro-2-cyano-3-dimethylamino-4'-fluoroacrylanilide as colorless needles, m.p. 155.5°-156.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04393217 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-ed5255fb38084eaf9f39eb8bd31e9fcc |
| Source note | uspto-grants-1983_07 |