1,1-Dimethoxyethyl(dimethyl)amine → HCID 70534846, compound

HRID 1074604Notes

Reaction equation

HRID 1074604 reaction equation
[C:1]([CH2:3][C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH2:13][CH3:14])=[O:5])#[N:2].CO[C:17](OC)([N:19]([CH3:21])[CH3:20])[CH3:18]>>[C:1](/[C:3](=[C:17](/[N:19]([CH3:21])[CH3:20])\[CH3:18])/[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH2:13][CH3:14])=[O:5])#[N:2]

Participants

3

Reactant 2

HCID 878351,1-Dimethoxyethyl(dimethyl)amineHCID 7318832-cyano-N-(2-ethylphenyl)acetamide

Product 1

HCID 70534846HCID 70534846, compound

Procedure

As for Example 1, 2-cyano-2'-ethylacetanilide is heated with N,N-dimethylacetamide dimethylacetal to give 2-cyano-3-dimethylamino-2'-ethylcrotonanilide as colorless prisms, m.p. 79°-81.5° C.

Sources & evidence

ORD record
ord-426a7bef687844508f5f155957ada7fb
Source dataset
uspto-grants-1983_07
Patent number
US04393217

Reaction notes

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