1,1-Dimethoxyethyl(dimethyl)amine → HCID 70536413, compound

HRID 1074605Notes

Reaction equation

HRID 1074605 reaction equation
[C:1]([CH2:3][C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH:13]([CH3:15])[CH3:14])=[O:5])#[N:2].CO[C:18](OC)([N:20]([CH3:22])[CH3:21])[CH3:19]>>[C:1](/[C:3](=[C:18](/[N:20]([CH3:22])[CH3:21])\[CH3:19])/[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH:13]([CH3:15])[CH3:14])=[O:5])#[N:2]

Participants

3

Reactant 2

HCID 878351,1-Dimethoxyethyl(dimethyl)amineHCID 3465225HCID 3465225, compound

Product 1

HCID 70536413HCID 70536413, compound

Procedure

As for Example 1, 2-cyano-2'-isopropylacetanilide, off-white crystals, m.p. 74°-78° C. (prepared by the procedure described in U.S. Pat. No. 3,116,312), is heated with N,N-dimethylacetamide dimethylacetal to yield 2-cyano-3-dimethylamino-2'-isopropylcrotonanilide as colorless prisms, m.p. 119°-121° C.

Sources & evidence

ORD record
ord-4a2fd17b923e41f39038038a09e12b67
Source dataset
uspto-grants-1983_07
Patent number
US04393217

Reaction notes

Loading…