Thiophenol → HCID 15478590, compound

HRID 1074932Notes

Reaction equation

[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH3:9][C:10]1[N:15]=[C:14]([CH2:16]Cl)[CH:13]=[CH:12][CH:11]=1.[O-]CC.[Na+]>>[CH3:16][C:14]1[CH:13]=[CH:12][CH:11]=[C:10]([CH2:9][S:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[N:15]=1

Participants

Reactant 3

HCID 7969Thiophenol

HCID 765456-Chloromethyl-2-methylpyridinium chloride

HCID 2723922Sodium ethoxide

Product 1

HCID 15478590HCID 15478590, compound

Procedure

Following the method of Example 1A thiophenol is reacted with 6-methyl-2-picolyl chloride hydrochloride in the presence of sodium ethoxide to give 2-methyl-6-((phenylthio)methyl)pyridine.

Sources & evidence

ORD record: ord-188ae8eea0074f51b983d89e334ad47d
Source dataset: uspto-grants-1983_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04394509

Reaction notes

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