Methylamine → HCID 178482513, compound

HRID 1075072Notes

Reaction equation

HRID 1075072 reaction equation
CO[C:3]1[C:7](OC)=[N:6][S:5](=[O:11])(=[O:10])[N:4]=1.[CH3:12][N:13]([CH2:15][C:16]1[N:21]=[C:20]([CH2:22][S:23][CH2:24][CH2:25][NH2:26])[CH:19]=[CH:18][CH:17]=1)[CH3:14].[CH3:27][NH2:28]>>[CH3:14][N:13]([CH2:15][C:16]1[N:21]=[C:20]([CH2:22][S:23][CH2:24][CH2:25][NH:26][C:3]2[C:7]([NH:28][CH3:27])=[N:6][S:5](=[O:11])(=[O:10])[N:4]=2)[CH:19]=[CH:18][CH:17]=1)[CH3:12]

Participants

4

Reactant 3

HCID 6329MethylamineHCID 122305383,4-Dimethoxy-1,2,5-thiadiazole 1,1-dioxideHCID 212920152-[(6-Dimethylaminomethyl-2-pyridyl)methylthio]ethylamine

Product 1

HCID 178482513HCID 178482513, compound

Procedure

When a methanolic solution of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is successively treated with an equimolar amount of 2-[(6-dimethylaminomethyl-2-pyridyl)methylthio]ethylamine [prepared in Example 136, Step C] and excess methylamine, the title compound is thereby produced.

Sources & evidence

ORD record
ord-94a89c2024ff48a98880b244f1982fd7
Source dataset
uspto-grants-1983_07
Patent number
US04394508

Reaction notes

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