HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 178477361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 5-Fluoro-4-thiouracil | HCID 2781213 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178477361 | HCID 178477361 | 70% |
Reaction Steps
The potassium salt of 5-fluoro-4-thiouracil (0.0065 mol) and ethyl iodide (0.014 mol) in methanol (40 ml) were stirred at room temperature for 6 days. The solutions were concentrated at reduced pressure and water (6 ml) added. The slowly precipitated product was recrystallised from water; yield 70%, m.p. 168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04395406 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-efc4cf14311f45f3a108de1fe99d8dba |
| Source note | uspto-grants-1983_07 |