HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178526043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178473171 | HCID 178473171 | — |
| Solvent | Potassium Hydroxide | HCID 14797 | — |
| Product | HCID 178526043 | HCID 178526043 | 41% |
Reaction Steps
4-Ethoxycarbonylmethylthio-5-fluoropyrimid-2-one (0.0013 mol) in 2 M potassium hydroxide (4 ml) was heated on a waterbath for 5-6 min. The solution was allowed to cool before neutralisation with dilute hydrochloric acid. The precipitated solid was recrystallised from methanol: yield 41%, m.p. 255° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04395406 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-d9ba412572a149cb87ceef334b74ce45 |
| Source note | uspto-grants-1983_07 |