2-Mercaptobenzoic Acid → HCID 12763557, compound

HRID 1075181Notes

Reaction equation

HRID 1075181 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]Cl)=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2].[SH:16][C:17]1[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=1[C:19]([OH:21])=[O:20]>>[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][S:16][C:17]2[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=2[C:19]([OH:21])=[O:20])=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 54432-Mercaptobenzoic AcidHCID 127635554-Nitro-2-trichloromethylbenzenesulfenyl chloride

Product 1

HCID 12763557HCID 12763557, compoundYield 87.1%

Procedure

61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride are reacted with 32 g of 2-mercaptobenzoic acid by a method similar to that of Example 1. 74 g (87% of theory) of o-(4-nitro-2-trichloromethylphenyldithio)-benzoic acid of melting point 224° C., are obtained.

Sources & evidence

ORD record
ord-697aa4b81ce14a2d9e4e4381a134cc21
Source dataset
uspto-grants-1983_07
Patent number
US04395415

Reaction notes

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