HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mercaptobenzoic Acid → HCID 12763557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mercaptobenzoic Acid | HCID 5443 | — |
| Reactant | 4-Nitro-2-trichloromethylbenzenesulfenyl chloride | HCID 12763555 | — |
| Product | HCID 12763557 | HCID 12763557 | 87.1% |
Reaction Steps
61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride are reacted with 32 g of 2-mercaptobenzoic acid by a method similar to that of Example 1. 74 g (87% of theory) of o-(4-nitro-2-trichloromethylphenyldithio)-benzoic acid of melting point 224° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04395415 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-697aa4b81ce14a2d9e4e4381a134cc21 |
| Source note | uspto-grants-1983_07 |