Methyl Bromide → HCID 12951712, compound

HRID 1075197Notes

Reaction equation

HRID 1075197 reaction equation
[CH3:1][N:2]([CH2:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][CH:9]=1)[CH3:3].[CH3:16][Br:17]>>[Br-:17].[CH3:3][N+:2]([CH2:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:9]=[CH:10][C:11]([O:14][CH3:15])=[CH:12][CH:13]=1)([CH3:16])[CH3:1]

Participants

3

Reactant 2

HCID 6323Methyl BromideHCID 12951640HCID 12951640, compound

Product 1

HCID 12951712HCID 12951712, compound

Procedure

N,N-Dimethyl-4-(4-methoxyphenyl)butylamine (4.35 g.) was reacted with methyl bromide according to the procedure of Example 46 to provide 4.95 g. of N,N,N-trimethyl-4-(4-methoxyphenyl)butylammonium bromide, which was recrystallized from acetone and methanol. M.P. 166°-168° C.

Workup

  1. customto provide 4.95 g
  2. customof N,N,N-trimethyl-4-(4-methoxyphenyl)butylammonium bromide, which was recrystallized from acetone and methanol

Sources & evidence

ORD record
ord-d978b261cc15457cae232bef115883fd
Source dataset
uspto-grants-1983_07
Patent number
US04395410

Reaction notes

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