Ethyl Bromide → HCID 12951746, compound

HRID 1075206Notes

Reaction equation

HRID 1075206 reaction equation
[CH2:1]([N:3]([CH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:2].[CH2:19]([Br:21])[CH3:20]>>[Br-:21].[CH2:1]([N+:3]([CH2:10][CH2:11][CH2:12][C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1)([CH2:19][CH3:20])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:2]

Participants

3

Reactant 2

HCID 6332Ethyl BromideHCID 20494480HCID 20494480, compound

Product 1

HCID 12951746HCID 12951746, compound

Procedure

5.21 Grams of N-ethyl-N-n-hexyl-3-phenylpropylamine was placed in a 200 ml. round bottom flask. 100 Milliliters of ethyl bromide was added. The mixture was refluxed five days. Excess ethyl bromide was removed by evaporation in vacuo leaving as an oil N,N-diethyl-N-n-hexyl-3-phenylpropylammonium bromide.

Workup

  1. temperatureThe mixture was refluxed five days
  2. customExcess ethyl bromide was removed by evaporation in vacuo

Sources & evidence

ORD record
ord-e470d52d67ac4d2b902c8a8728d29822
Source dataset
uspto-grants-1983_07
Patent number
US04395410

Reaction notes

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