Dimethylamine → HCID 12785882, compound

Participants

Reaction Steps

5 ml of a solution of dimethylamine in methanol (content 30 g of dimethylamine in 100 ml) are added to 0.5 g of 7-chloro-5-phenyl-2-phenylcarbamoyloxyamino-3-phenyloxycarbonyloxy-3H-1,4-benzodiazepine in 10 ml of methanol, whilst stirring. The mixture is stirred for 5 hours at room temperature and water is added to it; the residue is filtered off and dried.

Provenance & Evidence