HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13061754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 13061753 | HCID 13061753 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 13061754 | HCID 13061754 | — |
Reaction Steps
To a suspension of 300 g 2-(N-isopropyl-N-carbomethoxyamino)-4-methyl-benzonitrile in 750 ml of ethanol and 234 ml 10N sodium hydroxide are added dropwise over 80 minutes 576 g of a 40% solution of hydrogen peroxide. The resulting clear solution is acidified with 195 ml of concentrated hydrochloric acid, whereupon the title compound precipitates, m.p. 250°-251°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04395550 |
| Source dataset | uspto-grants-1983_07 |
| ORD ID | ord-78ff9319128b4824b004d6edbe2fba76 |
| Source note | uspto-grants-1983_07 |