HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13124491, compound → HCID 15428308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13124491 | HCID 13124491 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15428308 | HCID 15428308 | — |
Reaction Steps
(3S,4S)-3-benzyloxycarbonylamino-4-acetoxy-azetidin-2-one (5.56 g, 20 mmole) was hydrogenated with 5.6 g of 10% palladium on activated carbon in ethyl acetate (120 ml) at 50 psi hydrogen pressure at room temperature for 1.5 hrs. After removal of catalyst by filtration, the deproteced (3S,4S)-3-amino-4-acetoxy-azetidin-2-one in ethyl acetate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05905076 |
| Source dataset | uspto-grants-1999_05 |
| ORD ID | ord-edd06687fb134f6dbb17c71e04de33d0 |
| Source note | uspto-grants-1999_05 |