HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131721274, compound → HCID 131721273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131721274 | HCID 131721274 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131721273 | HCID 131721273 | — |
Reaction Steps
Alanine-Ethanolamine-palmitate (AEP) was prepared by hydrogenation of Z-Ala-Ethanolamine-palmitate in a Parr hydrogenator in the presence of palladium on charcoal (10%) in ethanol. The removal of the benzyloxycarbonyl group was monitored by HPLC (System B). After removing the catalyst by filtration and evaporation of the solvent the title compound was obtained in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05906922 |
| Source dataset | uspto-grants-1999_05 |
| ORD ID | ord-7473f4ad173745db9fe1dca2c9fe43a7 |
| Source note | uspto-grants-1999_05 |